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Beilstein J. Org. Chem. 2008, 4, No. 42, doi:10.3762/bjoc.4.42
Graphical Abstract
Figure 1: Structure of zoledronic acid.
Scheme 1: Reported methods for the synthesis of imidazol-1-yl-acetic acid (3) [8-10].
Scheme 2: Preparation of imidazol-1-yl-acetic acid hydrochloride (6) and its conversion into zoledronic acid (...
Scheme 3: Suggested mechanism of TiCl4-mediated tert-butyl ester cleavage.